Journal
ORGANIC LETTERS
Volume 17, Issue 22, Pages 5714-5717Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b03042
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Funding
- National Natural Science Foundation of China [21132003, 21421062, 21372131]
- Specialized Research Fund for the Doctoral Program of Higher Education [20130031110017]
- Ministry of Education of China [B06005]
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A highly efficient direct C-H allylation reaction at the a position Of N-acyl/sulfonyl tetrahydroisoquinolines under mild conditions Was developed. The reaction was also suitable for allylation of other protected nitrogen containing heterocycles.Several interesting transformations of the products into valuable synthetic intermediates are featured with the successful total synthesis of (+/-)-crispine.
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