Journal
ORGANIC LETTERS
Volume 17, Issue 19, Pages 4686-4689Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b02056
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Funding
- Robert A. Welch Foundation [F-0038]
- NIH-NIGMS [RO1-GM093905]
- Center for Green Chemistry and Catalysis
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Using stereo- and site-selective C-H allylation and crotylation of unprotected diols, an intermediate in the synthesis of premisakinolide A (bistheonellic acid B) that was previously made in 16-27 (LLS) steps is now prepared in only nine steps. This fragment also represents a synthesis of C(19)-C(32) of the actin-binding macrodiolide swinholide A.
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