Journal
ORGANIC LETTERS
Volume 17, Issue 10, Pages 2554-2557Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b01049
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Funding
- JSPS KAKENHI [25410111]
- Grants-in-Aid for Scientific Research [15H00934, 25410111] Funding Source: KAKEN
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A new Julia-type methylenation reagent, 1-methyl-2-(methylsulfonyl)benzimidazole (1e), reacts with a variety of aldehydes and ketones in the presence of either NaHMLDS (-55 degrees C to rt) or t-BuOK (rt, 1 h) in DMF to give the corresponding terminal alkenes in high yields. The byproducts are easily removed, and the reaction conditions are mild and practical.
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