Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 13, Issue 19, Pages 5399-5406Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ob00438a
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Funding
- National Natural Science Foundation of China [21402116, 21202095, 21172139]
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A general and efficient synthesis of trifluoromethyl substituted 5-alkylidene-1,3-dioxolane using a silver salt and DBU cooperatively catalyzed nucleophilic addition/cyclization of propargylic alcohols and trifluoromethyl ketones is described. The procedure produced 5-alkylidene-1,3-dioxolane derivatives with good to excellent yields and can be used with a broad range of substrates.
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