Journal
JOURNAL OF HETEROCYCLIC CHEMISTRY
Volume 50, Issue 4, Pages 774-780Publisher
WILEY-BLACKWELL
DOI: 10.1002/jhet.1556
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Hydroxy (tosyloxy) iodobenzene (HTIB), a hypervalent iodine reagent, has been extensively used for oxidative transformations. We have developed a one-pot synthesis wherein aldoximes when reacted with alkynes in the presence of HTIB result in the direct formation of isoxazoles. This simple and straightforward reaction allows for ease of purification while leading to the formation of high purity 3,5-disubstituted isoxazoles in moderate yields.
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