Journal
JOURNAL OF HETEROCYCLIC CHEMISTRY
Volume 46, Issue 6, Pages 1355-1363Publisher
WILEY
DOI: 10.1002/jhet.244
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Funding
- National Natural Science Foundation of China [20802061]
- Natural Science Foundation [08KJD150019]
- Jiangsu Education Committee [08QLT001]
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A series of new highly substituted isoquinoline derivatives was obtained from the reaction of 2-(1-substituted piperidin-4-ylidene)malononitrile, benzaldehyde and malononitrile or cyanoacetate in ionic liquid at 50 degrees C. This novel procedure was different from the previous method in the synthesis of isoquinoline using pyridine fragment as reactant to construct benzene ring, and as well as had the advantages of one-pot, mild and environmentally benign. A possible mechanism was proposed based on the further experimental results.
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