Journal
JOURNAL OF HETEROCYCLIC CHEMISTRY
Volume 45, Issue 2, Pages 533-539Publisher
WILEY-BLACKWELL
DOI: 10.1002/jhet.5570450236
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Acetic acid is an inexpensive and environmentally friendly solvent for facile, clean and high-yielding aryl amination of cyanuric chloride with aromatic amines, including nitroanilines. Aryl amination in acetic acid medium and isolation protocol are greatly simplified as compared to previously reported procedures. Under proper conditions, it is possible to attach the same or different aniline residues in a controlled way to obtain in excellent yields symmetrical and unsymmetrical 1,3,5-triazine derivatives, respectively.
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