Journal
JOURNAL OF HAZARDOUS MATERIALS
Volume 280, Issue -, Pages 127-133Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jhazmat.2014.08.001
Keywords
SAW sensor; Ammonia; Co3O4; SiO2; Composite film
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Funding
- Fundamental Research Funds for the Central Universities [ZYGX2012J047]
- National Natural Science Foundation of China [U1330108, 11304032]
- China Academy of Engineering Physics [U1330108]
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Surface acoustic wave (SAW) sensors based on Co3O4/SiO2 composite sensing films for ammonia detection were investigated at room temperature. The Co3O4/SiO2 composite films were deposited onto ST-cut quartz SAW resonators by a sal-gel method. SEM and AFM characterizations showed that the films had porous structures. The existence of SiO2 was found to enhance the ammonia sensing property of the sensor significantly. The sensor based on a Co3O4/SiO2 composite film, with 50% Co3O4 loading, which had the highest RMS value (3.72), showed the best sensing property. It exhibited a positive frequency shift of 3500 Hz to 1 ppm ammonia as well as excellent selectivity, stability and reproducibility at room temperature. Moreover, a 37% decrease in the conductance of the composite film as well as a positive frequency shift of 12,500 Hz were observed when the sensor was exposed to 20 ppm ammonia, indicating the positive frequency shift was derived from the decrease in film conductance. (C) 2014 Elsevier B.V. All rights reserved.
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