Journal
JOURNAL OF HAZARDOUS MATERIALS
Volume 213, Issue -, Pages 161-166Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jhazmat.2012.01.071
Keywords
Green synthesis; Nanosilver; Hydrogen peroxide; Electro-catalysis; Sensors; FTIR
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Funding
- Department of Science and Technology
- Council of Scientific and Industrial Research [CSIR-SRF], Government of India [09/001/(0342)/2011/EMR-I]
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Present green synthesis is an efficient, easy-going, fast, renewable, inexpensive, eco-friendly and non-toxic approach for nanosilver formation, which offers numerous benefits over physiochemical approaches. The X-ray diffraction (XRD) pattern suggests the formation and crystallinity of nanosilver. The average particle size of silver nanoparticles was 8.25 +/- 1.37 nm as confirmed by transmission electron microscopy (TEM). The UV-vis absorption spectrum shows a characteristic absorption peak of silver nanoparticles at 410 nm. FTIR confirms Azadirachtin as reducing and stabilizing agent for nanosilver formation. In addition, the nanosilver modified electrode (Ag/GC) exhibited an excellent electro-catalytic activity toward the reduction of hydrogen peroxide (H2O2). The produced nanosilver is stable and comparable in size. These silver nanoparticles show potential applications in the field of sensors, catalysis, fuel cells and nanodevices. (C) 2012 Elsevier B.V. All rights reserved.
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