Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 131, Issue 11, Pages 1192-1197Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2010.06.009
Keywords
Monofluoroolefination; Monofluoroalkenes; Monofluoromethyl arylsulfone; Julia-Kocienski reaction
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Funding
- Loker Hydrocarbon Research Institute
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Monofluoromethyl 3 5-bis(trifluoromethyl)phenyl sulfone 1 was synthesized and employed in Julia-Kocienski fluoroolefination reaction with various ketones and aldehydes Optimal reaction conditions were found to be the treatment of substrates with KOH or CsF in DMSO at room temperature Mixtures of (E) and (Z) isomers of monofluoroalkenes 4 were obtained in moderate to excellent yields (C) 2010 Elsevier B V All rights reserved
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