Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 131, Issue 8, Pages 879-882Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2010.04.010
Keywords
Thiourea; Fluorous organocatalyst; Reductive amination; Fluorous solid phase extraction (F-SPE)
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Funding
- Ministry of Education of China [200802881024]
- National Natural Science Foundation of China [20902047]
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A commercially available perfluorooctyl aniline and phenyl isothiocyanate were reacted under mild conditions to give 1-[4-(perfluorooctyl)phenyl]-3-phenylthiourea as an analogue of thiourea-based organocatalyst. This fluorous organocatalyst was successfully employed to direct reductive amination of aldehydes. It could be readily separated from reaction product by fluorous solid phase extraction for direct use. (C) 2010 Elsevier B.V. All rights reserved.
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