Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 130, Issue 8, Pages 742-748Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2009.05.018
Keywords
Crystal morphology; Hydrothermal synthesis; Fluoride; Perovskites; Photoluminescence
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Funding
- National Natural Science Foundation of China [20371044, 20621061]
- 973 Projects of China
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Micropolyhedra, microspheres and hollow microspheres of the cubic KMnF3 were selectively prepared by controllable, hydrothermal method at 120 degrees C. Manganese acetate and potassium fluoride were employed as the starting materials in the reaction, and variety of polyethylene glycol and dosage of citric acid were demonstrated to be responsible for the shape evolution. The samples were characterized by Xray diffraction, scanning electron microscopy, X-ray photoelectron spectra, UV-vis absorption spectroscopy and photoluminescence spectra. A possible mechanism for the growth of KMnF3 microcrystal was proposed. (C) 2009 Elsevier B.V. All rights reserved.
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