Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 129, Issue 10, Pages 994-997Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2008.04.008
Keywords
Copper(II) hexafluoroantimonate; Intramolecular Cannizzaro reaction; Phenylglyoxal; Double asymmetric induction; Anhydrous; Bis(oxazoline)
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Funding
- Toray Science Foundation
- G-COE in Chemistry, Nagoya
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The use of anhydrous phenylglyoxal provides a solution to the problem of low reactivity in the asymmetric intramolecular Cannizzaro reaction with alcohols. Double asymmetric induction was achieved in the reaction of anhydrous phenylglyoxal with D-(+)-menthol promoted by a (SS)-t-BuBox center dot copper(II) hexafluoroantimonate complex. (C) 2008 Elsevier B.V. All rights reserved.
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