Journal
JOURNAL OF CRYSTAL GROWTH
Volume 363, Issue -, Pages 1-6Publisher
ELSEVIER
DOI: 10.1016/j.jcrysgro.2012.09.029
Keywords
Floating zone technique; Single crystal growth; Metals
Funding
- Deutsche Forschungsgemeinschaft [SFB 609]
- Emmy Noether programme [WU595/3-1]
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The floating-zone growth of massive intermetallic single crystals is very often unsuccessful due to unfavorable solidliquid interface geometry and insufficient mixing of the melt which depends on the flow in the molten zone. A tailored magnetic two-phase stirrer system with radio frequency (RF) heating has been developed which enables the control of the melt flow by a significant change of the flow field. The magnetic system was used for the crystal growth of the Heusler compound Mn3Si due to their interesting properties such an itinerant antiferromagnetic and incommensurate spin-density wave state. The grown crystals were oriented and cut to samples with the crystallographic orientations (100) and (110) normal to a plane. Measurements of the temperature dependence of magnetization and specific heat are discussed in terms of contributions of other thermodynamic phases and phase transitions. (C) 2012 Elsevier B.V. All rights reserved.
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