4.4 Article

Application of solution techniques for rapid growth of organic crystals

Journal

JOURNAL OF CRYSTAL GROWTH
Volume 314, Issue 1, Pages 163-170

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.jcrysgro.2010.10.139

Keywords

Supersaturated solutions; Single crystal growth; Organic compounds; Scintillator materials; Neutron detection; Pulse shape discrimination

Funding

  1. US Department of Energy by Lawrence Livermore National Laboratory [DE-AC52-07NA27344]
  2. US Department of Energy Office of Non-proliferation Research and Development [NA-22]

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Single crystals of a pure hydrocarbon, 1,3,5-triphenylbenzene, with properties suitable for high-energy neutron detection were grown from toluene solutions using slow evaporation and temperature reduction methods with growth rates up to 10 mm/day. Application of the rapid growth technique developed earlier for growth of large water-soluble crystals shows that crystals of aromatic compounds can be successfully grown from solutions in large volumes required for their use as scintillator materials for radiation detection. (C) 2010 Elsevier B.V. All rights reserved.

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