Journal
JOURNAL OF CRYSTAL GROWTH
Volume 321, Issue 1, Pages 162-166Publisher
ELSEVIER
DOI: 10.1016/j.jcrysgro.2011.02.036
Keywords
Alfa-boron; Single crystal growth; High pressure; Growth from melt
Funding
- German Science Foundation (DFG) [SPP1236, SPP1178]
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A method of synthesis of single crystals of alfa-boron (alpha-B) is presented. alpha-Boron has been crystallized from a boron-platinum melt at high pressures (6-11 GPa) and high temperatures (1200-1600 degrees C). The method is based on the high-pressure large volume (multi-anvil) press technique. An average size of the as-grown isometric crystals is 60-80 mu m in maximum dimension. A refinement of an accurate crystal structure of alpha-B against single crystal X-ray diffraction data demonstrates the excellent quality of the single crystals. The crystal structure is in good agreement with the literature. (C) 2011 Elsevier B.V. All rights reserved.
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