Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 63, Issue 4, Pages 713-720Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958970903502736
Keywords
Nanoparticle; Coordination polymer; Pb(II); PbO
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Funding
- Bonyade Melli Nokhbegan
- Tarbiat Modares University
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Microcrystals of a new Pb(II) coordination polymer, [Pb-2(1,3,5-HBTC)(2)(H2O)(4)]center dot H2O (1) (1,3,5-H3BTC = 1,3,5-benzentricarboxylic acid), was synthesized by a sonochemical method. The structure was characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses, and IR spectroscopy. Thermal stability was studied by thermal gravimetric and differential thermal analyses. After the calcination of nanosized 1 at 400 degrees C, pure phase nanosized Pb(II) oxide has been produced.
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