Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 61, Issue 22, Pages 3634-3641Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958970802101689
Keywords
Sschiff-base complexes; Macrocyclic complexes; Salicylaldehyde derivatives
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Six new macrocyclic complexes were synthesized by template reactions of salicylaldehyde derivatives with (+/-)-trans-1,2-diaminocyclohexane and metal(II) nitrates. The metal to ligand ratio was 1 : 1. The Cu(II) complexes are proposed to be square planar and the Ni(II) and Co(II) complexes are proposed to be tetrahedral. The complexes are 1 : 2 electrolytes as shown by their molar conductivities (M) in DMF. The metal complexes are characterized by elemental analyses, FT-IR, UV-Vis, magnetic susceptibility measurements, molar conductivity measurements and mass spectra.
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