Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 61, Issue 22, Pages 3666-3673Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958970802108809
Keywords
N-acetyl-L-cysteine; Palladium(II); C-13 NMR; Infrared spectroscopy; UV-Vis; Thermal analysis
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Funding
- FAPESP
- Sao Paulo State Research Foundation, Brazil [07/56317-1, 06/55367-2, 04/11106-5]
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Chemical and spectroscopic studies of a new palladium(II) N-acetyl-L-cysteine complex are described. Elemental analyses for the solid complex are consistent with the formula [Pd(C5H8NO3S)(2)] H2O or [Pd(NAC)(2)] H2O. Solid-state C-13 nuclear magnetic resonance (NMR), UV-Visible (UV-Vis) and infrared (IR) spectroscopic analyses are consistent with coordination of the ligand to palladium(II) through the nitrogen and sulfur atoms in a square-planar geometry. Thermogravimetric and differential thermal analyses confirmed the composition; final residue was identified as metallic palladium.
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