Journal
NEW JOURNAL OF CHEMISTRY
Volume 39, Issue 5, Pages 3341-3344Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4nj01822b
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- Department of Science and Technology, New Delhi under DST Woman Scientist Scheme [SR/WOS-A/CS-78/2011(G)]
- Department of Science and Technology, New Delhi
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A tetradentate Schiff base derived palladium complex has been developed as a catalyst for the room temperature Sonogashira reaction under copper free conditions. The main catalytic species, a Pd-complex was derived from Schiff base ligand N,N'-bis(salicylidene)-aryl-methanediamine and Pd(OAc)(2). Electron rich, electron deficient and sterically hindered aryl iodides underwent smooth coupling to afford good to excellent yield of diaryl alkynes in isopropanol at room temperature. The protocol is also suitable for aliphatic alkynes.
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