Journal
NEW JOURNAL OF CHEMISTRY
Volume 39, Issue 12, Pages 9605-9610Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5nj01914a
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Funding
- Department of Atomic Energy (DAE) Board of Research in Nuclear Sciences (BRNS), Mumbai, India [2012/37C/33/BRNS]
- UGC-CSIR, New Delhi, India
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In this paper, TiO2 fine particles, TiO2-P25, protonated trititanate (H2Ti3O7) nanorods and nanotubes were used as recyclable solid-acid catalysts for the solvent free synthesis of tertiary CL-aminophosphonates through Kabachnik Fields reaction. Among them, H2Ti3O7 nanotubes showed remarkable catalytic performance and it was due to strong and sufficient Lewis and Bronsted acid sites on a large nanotubular surface. More importantly, for the first time we reported some novel 5,8-dioxa-10-azadispiro[2.0.4.3]undecane bearing tertiary CL-aminophosphonates.
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