Journal
JOURNAL OF CHROMATOGRAPHY A
Volume 1296, Issue -, Pages 204-213Publisher
ELSEVIER
DOI: 10.1016/j.chroma.2013.03.020
Keywords
Solid phase analytical derivatization; Analytical derivatization; Sample preparation; Extractive alkylation; Phase transfer catalyst
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Analytical derivatization (AD) is an important procedure in analysis as it improves the sensitivity, selectivity and chromatographic separation. Solid phase analytical derivatization (SPAD) combines extraction and derivatization into a single step fulfilling many aspects of a good sample preparation technique, which includes low organic solvent consumption, economical, ease of automation with any chromatographic system and applicability in a wide range of complicated matrices. In this review we have focused on wide applications of SPAD when used in combination with different sample preparation methods, such as solid phase extraction, ion exchange resins, solid phase microextraction, in-tube, microfluidic devices, and hollow fiber extraction methods. (C) 2013 Elsevier B.V. All rights reserved.
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