Journal
JOURNAL OF CHROMATOGRAPHY A
Volume 1250, Issue -, Pages 99-104Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.chroma.2012.06.017
Keywords
3-MCPD fatty acid esters; Supercritical fluid chromatography; Triple quadrupole mass spectrometry
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We have established a high-throughput and sensitive analytical method based on supercritical fluid chromatography (SFC) coupled with triple quadrupole mass spectrometry (QqQ MS) for 3-monochloropropane-1,2-diol (3-MCPD) fatty acid esters in edible oils. All analytes were successfully separated within 9 min without sample purification. The system was precise and sensitive, with a limit of detection less than 0.063 mg/kg. The recovery rate of 3-MCPD fatty acid esters spiked into oil samples was in the range of 62.68-115.23%. Furthermore, several edible oils were tested for analyzing 3-MCPD fatty acid ester profiles. This is the first report on the analysis of 3-MCPD fatty acid esters by SFC/QqQ MS. The developed method will be a powerful tool for investigating 3-MCPD fatty acid esters in edible oils. (C) 2012 Elsevier B.V. All rights reserved.
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