Journal
JOURNAL OF BIOBASED MATERIALS AND BIOENERGY
Volume 3, Issue 1, Pages 108-111Publisher
AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/jbmb.2009.1004
Keywords
Biodiesel; Phosphitylation; P-31-NMR; Transesterification
Funding
- PSE Fellowship
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Phosphitylation of hydroxyl groups in biodiesel samples with 2-chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane followed by P-31-NMR analysis provides a rapid quantitative analytical technique for the determination of substitution patterns on partially esterified glycerols. The unique P-31-NMR chemical shift data was established with a series mono and di-substituted fatty acid esters of glycerol and then utilized to characterize an industrial sample of partially processed biodiesel.
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