Journal
JOURNAL OF APPLIED PHYSICS
Volume 116, Issue 3, Pages -Publisher
AMER INST PHYSICS
DOI: 10.1063/1.4890354
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Funding
- Slovak Research and Development Agency [APVV-0222-10, APVV-0132-11]
- VEGA projects of Ministry of Education of the Slovak Republic [1/0583/11, 1/0861/12]
- ERDF EU [ITMS 26220220105]
- DESY/HASYLAB [I-20110282 EC]
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One-dimensional (1D) chain-like nanocomposites, created by ensembles of nanoparticles of with diameter similar to 13 nm, which are composed of an iron core (similar to 4 nm) and a silica protective layer, were prepared by a self-assembly process. Chain-like Fe@SiO2 ensembles were formed due to strong magnetic dipole-dipole interactions between individual Fe nanoparticles and the subsequent fixation of the Fe particles by the SiO2 layers. X-ray near edge absorption spectra measurements at the Fe K absorption edge confirm that the presence of a silica layer prevents the oxidation of the magnetic Fe core. Strong magnetic interactions between Fe cores lead to long-range ordering of magnetic moments, and the nanoparticle ensembles exhibit superferromagnetic characteristics demonstrated by a broad blocking Zero-field cooling (ZFC)/field-cooling distribution, nearly constant temperature dependence of ZFC magnetization, and non-zero coercivity at room temperature. Low room-temperature coercivity and the presence of electrically insulating SiO2 shells surrounding the Fe core make the studied samples suitable candidates for microelectronic applications. (C) 2014 AIP Publishing LLC.
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