Journal
JOURNAL OF APPLIED PHYSICS
Volume 112, Issue 6, Pages -Publisher
AMER INST PHYSICS
DOI: 10.1063/1.4751332
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Funding
- Ministry of Sciences and Technology of China through the 973-Project [2009CB623301]
- National Science fund for Creative Research Groups [50921061]
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Using high resolution synchrotron x-ray diffraction, we systemically study the crystal structure evolution of nano BaTiO3 as function of temperatures and particle sizes. In the temperature range from 200 K to 450 K, the nano BaTiO3 with different particles in the range from 5 nm to 100 nm are phase coexisting. The phase fraction evolutions of different nano BaTiO3 indicated that there is an anomaly at particle size around 20 nm, a phase reentrance taking place. The competition of the shear stresses and the compressive stresses on the particle surface, and the delicate balance between them are responsible for the reentrance phenomenon. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.4751332]
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