Journal
JOURNAL OF APPLIED ELECTROCHEMISTRY
Volume 42, Issue 9, Pages 667-677Publisher
SPRINGER
DOI: 10.1007/s10800-012-0445-x
Keywords
Electrochemistry; Microreactors; Electrosynthesis; Fluorination; NADH regeneration; Optimization; Simulation; POISEUILLE; Pressure drop
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The study focuses on the design and construction, as well as the theoretical and experimental optimization of electrochemical filter press microreactors for the electrosynthesis of molecules with a high added value. The main characteristics of these devices are firstly a high-specific electrochemical area to increase conversion and selectivity, and secondly the shape and size of the microchannels designed for a uniform residence time distribution of the fluid. A heat exchanger is integrated into the microstructured electrode to rapidly remove (or supply) the heat required in exo- or endothermic reactions. The microreactors designed are used to perform-specific electrosynthesis reactions such as thermodynamically unfavorable reactions (continuous NADH regeneration), or reactions with high enthalpy changes.
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