Journal
JOURNAL OF APPLIED ELECTROCHEMISTRY
Volume 41, Issue 6, Pages 663-668Publisher
SPRINGER
DOI: 10.1007/s10800-011-0277-0
Keywords
Rh-Pd particles; Cyclic voltammetry; Amperometry; Hydrogen peroxide
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Funding
- National Science Council (NSC) of Taiwan (ROC)
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Electrochemical deposition method was employed for the fabrication of rhodium-palladium (Rh-Pd) particles on the glassy carbon electrode (GCE) and indium tin oxide (ITO) electrode surface. Surface morphological analysis of Rh-Pd film has been carried out using scanning electron microscopy (SEM) and X-ray diffraction (XRD) analysis. Here, the electrodeposited Rh-Pd particles were found in the average size range of 30-200 nm. The electrochemical activities of the Rh-Pd film have been investigated using cyclic voltammetry (CV) and electrochemical impedance spectroscopic (EIS) analysis. The Rh-Pd particles-modified GCE successfully detects the hydrogen peroxide (H2O2) (in pH 7.0 phosphate buffer solution (PBS)) in the linear range in the lab (10-460 mu M) and real samples (10-340 mu M). The Rh-Pd particles-modified GCE possesses the good sensitivity and selectivity for the detection of H2O2 in lab and real samples.
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