Journal
JOURNAL OF APPLIED CRYSTALLOGRAPHY
Volume 44, Issue -, Pages 558-568Publisher
WILEY-BLACKWELL
DOI: 10.1107/S0021889811007527
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Funding
- Atomic Energy Initiative, MEXT, Japan
- Grants-in-Aid for Scientific Research [22245018] Funding Source: KAKEN
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The small-angle neutron scattering spectrometer SANS-U at the research reactor (JRR-3) of the Japan Atomic Energy Agency, Tokai, Japan, has been successfully upgraded. This major upgrade was undertaken in order to install a high-resolution position-sensitive detector consisting of a cross-wired position-sensitive photomultiplier tube combined with a ZnS/(6)LiF scintillator on the SANS-U spectrometer. Without changing the total length of the spectrometer, the aim was to extend the accessible low-Q limit (Q is the magnitude of the scattering vector) and to shorten the measurement time by employing focusing small-angle neutron scattering (FSANS). By using both spherical MgF(2) biconcave lenses and the new high-resolution position-sensitive detector, the accessible low-Q limit was extended from 2.5 x 10(-3) to 3.8 x 10(-4) angstrom(-1). As a result, SANS-U can continuously cover a wide Q range from 3.8 x 10(-4) to 0.35 angstrom(-1) with a wavelength of 7 angstrom. FSANS can be utilized not only to improve the accessible low-Q limit but also to increase the intensity of incident neutrons passing through the sample in the conventional Q range from 2.5 x 10(-3) to 0.35 angstrom(-1). The use of 'high-intensity' FSANS also allowed a reduction of the measuring time by approximately 1/3.16 by increasing the incident neutron intensity.
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