Journal
JOURNAL OF ANALYTICAL CHEMISTRY
Volume 67, Issue 12, Pages 960-966Publisher
PLEIADES PUBLISHING INC
DOI: 10.1134/S1061934812120040
Keywords
atropine; scopolamine; HPLC; GC; analytical scenario for the determination of tropane alkaloids
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Funding
- Federal State Program Investigations and Projects on High-Priority Directions of the Development of Scientific and Technical Complex in Russia [16.552.11.7013]
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An analytical scenario has been developed for the determination of some tropane alkaloids in Datura metel, including sample preparation by solid-phase extraction and chromatographic (GC and HPLC) determination of the analytes. The proposed scenario is rapid and provides the complete recovery of alkaloids; the analytical range for atropine and scopolamine is 0.01-30 mg/mL. The procedure ensures the simultaneous determination of compounds from other classes of substances.
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