4.2 Article

Determination of Impurities in High-Purity Hydrogen Sulfide by Gas Chromatography-Mass Spectrometry using Gas Adsorption Capillary Columns

Journal

JOURNAL OF ANALYTICAL CHEMISTRY
Volume 66, Issue 6, Pages 634-640

Publisher

MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1061934811060104

Keywords

hydrogen sulfide; impurities; gas chromatography-mass spectrometry; capillary columns; detection limit

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Gas chromatography-mass spectrometry has been used to study the impurity composition of high-purity hydrogen sulfide. Impurities of atmospheric gases, COS, CS(2), SO(2), benzene, toluene, thiophene, and its homologues have been detected. Detection limits of impurities are 10(-7)-10(-5) vol %.

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