Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 496, Issue 1-2, Pages 638-643Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2010.02.152
Keywords
Nanocrystalline materials; Tin dioxide; Inorganic precursors; Photoluminescence
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Funding
- council of Iran National Science Foundation
- University of Kashan
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The present investigation reports the synthesis of SnO2 nanoparticle using thermal decomposition and characterization of their physicochemical characterization. The SnO2 nanoparticle powder has been prepared using [bis(2-hydroxyacetophenato)tin(II)], [Sn(HAP)(2)]; as precursor. Transmission electron microscopy (TEM) analysis was demonstrated that SnO2 nanoparticle with an average diameter of about 14-22 nm. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM). Fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA), X-ray photoelectron spectroscopy (XPS) and photoluminescence (PL) spectroscopy. Also the novel precursor was thermal treated in solid-state reaction in different temperature, 350, 450, and 550 degrees C. (C) 2010 Elsevier B.V. All rights reserved.
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