Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 476, Issue 1-2, Pages 797-801Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2008.09.121
Keywords
Nanoparticles; Ni; Inorganic materials; Characterization methods; Chemical synthesis
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Funding
- council of University of Kashan
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The present investigation reports, the novel synthesis of nanoparticles Ni and NiO using thermal decomposition and their physicochemical characterization. The nanoparticles Ni powder have been prepared using [bis(2-hydroxyacetophenato)nickel(II)] as precursor. Transmission electron microscopy (TEM) analysis was demonstrated nanoparticles Ni with an average diameter of about 14-22 nm. The products were characterized by X-ray diffraction (XRD),TEM, high-resolution transmission electron microscopy(HRTEM) and Fourier transform infrared (FT-IR) spectroscopy. The magnetic property of Ni and NiO was studied with vibrating sample magnetometer (VSM). (C) 2008 Elsevier B.V. All rights reserved.
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