Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 481, Issue 1-2, Pages 438-445Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2009.03.002
Keywords
Ceramic-matrix composites (CMCs); Physical properties
Categories
Funding
- Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)
- Fundacao Cearense de Apoio ao Desenvolvimento Cientifico e Tecnologico (FUNCAP)
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq)
- U.S. Air Force Office of Scientific Research (AFOSR) [FA9550-08-1-0210]
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The structural properties of a magneto-dielectric composite based on the polycrystalline phases (Cr0.75Fe1.25O3) CRFO100 and (Fe0.5Cu0.75Ti0.75O3) FCTO100, synthesized by the mixed oxide solid-state reaction methodology, have been investigated in this paper. The constituent phases, as well their composite series (Cr0.75Fe1.25O3)([W])-(Fe0.5Cu0.75Ti0.75O3)([100-W]), for W = 0, 17, 34, 50, 66, 83 and 100, were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDXS), and Fe-57 Mossbauer spectroscopy techniques. The identification and subsequent refinement of XRD data revealed for CRFO100 and FCTO100 trigonal and cubic structures, respectively. The Mossbauer spectra related to the composites signalize a probable paramagnetic doublet due to FCTO100 phase, and a magnetic sextet due to CRFO100 phase, both associated with Fe3+ in octahedral coordination. (C) 2009 Elsevier B.V. All rights reserved.
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