Journal
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume 62, Issue 51, Pages 12462-12470Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jf5036838
Keywords
mycotoxins feed; farmed fish; beauvericin; enniatins
Funding
- Spanish Ministry of Economy and Competitiveness [AGL2013/43194/P]
- Valencian government, Spain [PLAT/2009-012]
- Universitat de Valencia [UV-BI-12-007]
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A new analytical method for the simultaneous determination of enniatins (ENs) and beauvericin (BEA) in fish feed and fish tissues by liquid chromatography coupled to mass spectrometry with linear ion trap (LC-MS/MS-LIT) was developed. Results showed that the developed method is precise and sensitive. The presence of emerging Fusarium mycotoxins, ENs and BEA, was determined in samples of aquaculture fish and feed for farmed fish, showing that all feed samples analyzed were contaminated with mycotoxins, with 100% coexistence. In aquacultured fish samples, the highest incidence was found in edible muscle and liver. As for the exposure assessment calculated, it was found that average consumer intake was lower than tolerable daily intake (TDI) values for other Fusarium mycotoxins.
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