Journal
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume 61, Issue 33, Pages 7889-7895Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jf4014718
Keywords
sheath-flow probe electrospray ionization mass spectrometry; pesticide analysis; real-time
Funding
- Japan Science and Technology Agency (JST)
- Japan Society for the Promotion of Science (JSPS)
- Grants-in-Aid for Scientific Research [13F03034] Funding Source: KAKEN
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For the real time and direct analysis of chemical constituents from living beings and dry sample, sheath-flow probe electrospray ionization mass spectrometry (SF-PESI-MS) has been newly developed. The components from dry or semidry biological tissues can be extracted using the solvent and picked up by the needle for electrospray. This technique was applied to real-time pesticide analysis of living plants. The results have been validated with that of a well-known system, liquid extraction surface analysis mass spectrometry (LESA-MS). It is demonstrated that SF-PESI-MS can produce reasonable ionization efficiency, which is confirmed by LESA-MS.
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