Journal
NANO
Volume 10, Issue 8, Pages -Publisher
WORLD SCIENTIFIC PUBL CO PTE LTD
DOI: 10.1142/S179329201550112X
Keywords
Carbon nanotubes; structural improvement; CVD; thermite; field emission
Funding
- Natural Science Foundation of Jiangsu Province, China [BK20140870]
- National Natural Science Foundation of China [11304159]
- NUPTSF [NY213078, NY214045]
- Science and Technology Innovation Training Program (STITP) of Nanjing University of Posts and Telecommunications
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Multi-walled carbon nanotubes (MWCNTs) produced by chemical vapor deposition (CVD) are the most common commercial products at extremely low price in the market. However, due to the inherent drawbacks of CVD surroundings at temperature below similar to 1000 degrees C, CVD-grown nanotubes usually have very disordered structure, resulting in most of their properties being much below expectations. Herein, we present a simple and energy-efficient method for improving rapidly the structure of CVD-grown MWCNTs via a drastic thermite reaction process. Direct observations from scan electron microscope (SEM) and transmission electron microscope (TEM) images, decrease of /D//G ratios in Raman spectra, increase of the starting oxidation temperatures observed in thermogravimetric analysis (TGA), decrease of the volumetric electrical resistivity and decrease of the turn-on electric fields from 3.64 to 2.88 V/mu m in field emission measurements suggest that the graphitization of MWCNTs can be effectively enhanced and the structure of nanotubes becomes more ordered after the drastic thermite reaction process.
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