Journal
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume 58, Issue 1, Pages 513-519Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jf902264y
Keywords
In situ monitoring; NMR; rennet coagulation; syneresis; casein; slicing
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The objective of this study was to monitor rennet-induced milk gel formation and mechanically induced gel syneresis in situ by low-field NMR. pH, temperature, and gel firmness at cutting time were varied in a factorial design. The new curve-fitting method Doubleslicing revealed that during coagulation two proton populations with distinct transverse relaxation times (T-2,T-1 = 181, T-2,T-2 = 465 ms) were present in fractions (f(1) = 98.9%, f(2) = 1.1%). Mechanical cutting of the gel in the NMR tube induced macrosyneresis, which led to the appearance of an additional proton population (T-2,T-3 = 1500-2200 ms) identified as whey. On the basis of NMR quantification of whey water the syneresis rate was calculated and found to be significantly dependent on pH and temperature.
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