Journal
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE
Volume 46A, Issue 7, Pages 2947-2955Publisher
SPRINGER
DOI: 10.1007/s11661-015-2898-0
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Funding
- EPRI's Technology Innovation Program on Advanced Materials
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In a number of nickel-based superalloy systems strengthened by gamma prime (gamma'), eta-phase (Ni3Ti, eta) forms during prolonged high-temperature exposure, but its effect on mechanical properties is not well characterized. Using thermodynamic modeling and design-of-experiments techniques, three modifications of the nickel-based superalloy Nimonic (Nimonic(A (R)) is a trademark of Special Metals Corporation group of companies.) 263 were identified that yield increased volume fractions of the eta-phase (Ni3Ti, eta) at temperatures above 1023 K (750 A degrees C). Volume fractions of eta-phase were evaluated for each alloy and heat-treatment condition using optical microscopy, scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction. Compared to Nimonic 263, small additions of V and Ta were found to increase the volume fraction of eta-phase above 1023 K (750 A degrees C) from approximately 5 pct to above 15 pct, thus providing a route for future mechanical behavior experimental studies, which was not in the scope of this work.
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