Journal
INORGANICA CHIMICA ACTA
Volume 362, Issue 10, Pages 3427-3432Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.ica.2009.03.040
Keywords
Manganese(II); Nanoparticle; Sonochemical; Thermal analysis
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Funding
- Zanjan and Tarbiat Modares Universities
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Nano-scale and single crystals of a new Mn-II complex, {[Mn(pyterpy)(H2O)(NCS)(1.88)Cl-0.12] center dot DMF} (1) [pyterpy = 4'-(4-pyridyl)-2,2':6',2 ''-terpyridine] have been synthesized by the reaction of pyterpy and mixtures of manganese(II) acetate and potassium thiocyanate as well as potassium chloride using sonochemical and heat gradient methods, respectively. The nano-structure was characterized by IR spectroscopy and scanning electron microscopy (SEM), and the structure of compound 1 was determined by single-crystal X-ray diffraction. Thermal stability and catalytic properties of nanoparticles and single crystalline samples of compound 1 were studied and are compared with each other. (C) 2009 Elsevier B.V. All rights reserved.
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