Journal
INORGANIC MATERIALS
Volume 48, Issue 5, Pages 494-499Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0020168512050214
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- Russian Foundation for Basic Research [09-03-01067]
- RF Ministry of Education and Science [14.740.11.0281]
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The effect of sonication on the composition and properties of zirconia precipitated from aqueous zirconyl nitrate solutions at various pH values has been studied using thermal analysis, X-ray diffraction, and low-temperature nitrogen adsorption measurements. The results demonstrate that acoustic processing considerably reduces the content of sorbed ions in amorphous ZrO2 center dot xH(2)O gels and allows one to control the composition and microstructure of the nanocrystalline zirconia produced through thermal decomposition of the gels.
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