Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 40, Issue -, Pages 129-132Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.inoche.2013.11.026
Keywords
Alkalinity regulator; Framework Ti content; Crystal morphology
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Funding
- National Basic Research Program of China [2011CB808703, 2012CB821700]
- 111 project [B07016]
- KAUST [CRG-1-2012-LAI-009]
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A new method to synthesis TS-1 has been developed using the carbon dioxide (CO2) as an alkalinity regulator that resulted in the increased framework Ti contents. The prepared catalyst had a Si/Ti ratio as low as 40 in contrast to the ratio of 56 prepared through conventional synthesis. The twin crystals with the length of 2 mu m were formed via introduction of CO2. The catalytic activity of TS-1 is remarkably enhanced compared with the conventional synthesis. (C) 2013 Elsevier B.V. All rights reserved.
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