Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 15, Issue -, Pages 163-166Publisher
ELSEVIER
DOI: 10.1016/j.inoche.2011.10.015
Keywords
Palladium; Tellurium ligand; Synthesis; Structure; Nano-particle; Heck coupling
Categories
Funding
- Council of Scientific and Industrial Research (India) [01(2421)10/EMR-II]
- University Grants Commission (India)
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The complexes, [PdCl2(L)] (1-2) (L = N-{2-(aryltelluro)ethyl}morpholine/piperidine) have been synthesized and characterized by multi-nuclei NMR and single crystal X-ray crystallography. They on reaction with aryl chloride/bromide and morpholine/piperidine give similar to 5 nm size nano-particles of PdTe. The 0.005 mol% of 2 is suitable for Heck coupling (conversion up to 93%). (C) 2011 Elsevier B.V. All rights reserved.
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