Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 12, Issue 11, Pages 1150-1153Publisher
ELSEVIER
DOI: 10.1016/j.inoche.2009.09.008
Keywords
Metal sulfonate; MOF; Layered compound; Organic linkers; Hydrothermal synthesis
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Funding
- Center for Applied Research (CAR) in Valdosta State University (VSU)
- NSF-DBI [0420454]
- NSF
- University of Florida
- Div Of Biological Infrastructure
- Direct For Biological Sciences [0420454] Funding Source: National Science Foundation
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A rare two-dimensional layered inorganic-organic hybrid material, strontium sulfonate Sr[C2H4(SO3)(2)] was synthesized by hydrothermal reaction of strontium chloride hexahydrate and ethane disulfonic acid at 160 C. Single-crystal X-ray diffraction was utilized for structural determination. Data showed that the compound, crystallized in the monoclinic system and space group of C2/c. With cell parameters a = 8.3183(7) angstrom, b = 5.4416(5) angstrom and c = 14.9784(13) angstrom. The new material was extensively studied by DRIFT-infrared spectroscopy, thermogravimetric analysis, SEM and powder X-ray diffraction. Results show that the compound is thermally stable. (c) 2009 Elsevier B.V. All rights reserved.
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