Journal
INORGANIC CHEMISTRY
Volume 57, Issue 16, Pages 9844-9850Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.inorgchem.8b00685
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Funding
- Polish Ministry of Science and Higher Education through the project Diamentowy Grant [D12015 019445]
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The reduction of cobalt molybdenum oxide under an ammonia atmosphere resulting in the formation of ternary interstitial nitride Co3Mo3N was studied. Intermediate phases were identified by an in situ powder X-ray diffraction using a reaction chamber. It was supplemented by a thermogravimetric analysis of the process. The presence of intermediate phases, CoMoO4, Co2Mo3O8, Mo2N, metallic cobalt, and Co2Mo3N, was observed. A synthesis route of Co3Mo3N by an ammonolysis method was proposed.
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