Journal
INORGANIC CHEMISTRY
Volume 51, Issue 4, Pages 2186-2190Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic202147h
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Funding
- NNSFC [20901064, 20825103, 21021061, 90922031]
- Ministry of Science and Technology of China [2012CB821704]
- Fundamental Research Funds for the Central Universities [2010121016]
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A pentanuclear dysprosium cluster, [Dy-5(mu(3)- OH)(6)(Acc)(6)(H2O)(10)]center dot Cl-9 center dot 24H(2)O (1), has been synthesized through the reaction of 1-amino-cyclohexanel-carboxylic acid (Acc) and DyCl3 center dot 5H(2)O. Crystal structural analysis reveals that the metal core of cluster 1 shows an unprecedented trigonal bipyramidal (TBP) geometry. Magnetic studies indicate that the Dy-5 cluster exhibits slow magnetic relaxation.
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