Journal
INORGANIC CHEMISTRY
Volume 49, Issue 4, Pages 1674-1678Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic902081r
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Funding
- National Natural Science Foundation of China [20771098]
- Fund for Creative Research Groups [20921002]
- National Basic Research Program of China [2007CB935502, 2006CB601103]
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Sr-5(PO4)(3)Cl:Eu2+ nanorod bundles were successfully prepared through a facile hydrothermal method, The X-ray diffraction (XRD) and FT-IR results demonstrate that the product is a pure hexagonal phase of Sr-5(PO4)(3)Cl. The scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution TEM (HRTEM) images indicate that the as-prepared Sr-5(PO4)(3)Cl:Eu2+ nanorod bundles consist of parallel nanorods with diameters ranging from 20 to 30 nm and that the nanorods row along the [002] direction. The photoluminescence spectra show that the Eu3+ ions have been reduced to Eu2+ ions successfully and that the as-obtained Sr-5(PO4)(3)Cl:Eu2+ phosphor exhibited intense blue emission. Furthermore, this new simple synthetic route may be of much significance in the synthesis of other divalent europium ions activated nanoscale phosphors by aqueous method.
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