Journal
INORGANIC CHEMISTRY
Volume 49, Issue 23, Pages 10756-10758Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic1018532
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Funding
- Office of Vehicle Technologies, of the U.S. Department of Energy [DE-AC02-05CH11231, 6878940]
- NSF [CHE 0541766]
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The novel organophosphorus-containing lithium salt Li(THF)-[(C2O4)B(O2PPh2)(2)] (1; THF = tetrahydrofuran) was synthesized and characterized using a variety of spectroscopic techniques. An X-ray structural analysis on crystals of 1 grown from THF reveals a dimeric structure [Li(THF)(C2O4)B(O2PPh2)(2)](2)center dot THF, whereby the two units of 1 are bridged via P-O ... Li interactions. Compound 1 displays high air and water stability and is also thermally robust, properties needed of electrolytes for their possible use as electrolytes and/or additives in lithium-ion battery applications.
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