Journal
INDUSTRIAL CROPS AND PRODUCTS
Volume 36, Issue 1, Pages 401-404Publisher
ELSEVIER
DOI: 10.1016/j.indcrop.2011.09.015
Keywords
Supercritical CO2; Cannabis sativa L.; Hempseed oil; FAME analysis; PUFA's; Oxidation stability
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Funding
- Friuli-Venezia Giulia Region [art. 17, LR 26/2005]
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Supercritical carbon dioxide (SC-CO2) was employed to extract oil from hemp (Cannabis sativa L.) seeds. For ground seeds, the supercritical extraction was carried out at temperatures of 40, 60 and 80 degrees C and pressures of 300 and 400 bar. Different solvent-ratios were applied. Supercritical CO2 extractions were compared with a conventional technique, n-hexane in Soxhlet. The extraction yields, fatty acid composition of the oil and oxidation stability were determined. The seed samples used in this work contained 81% PUFAs, of which 59.6% was linoleic acid (omega-6), 3.4% gamma-linolenic (omega-3), and 18% alpha-linolenic (omega-6). The highest oil yield from seeds was 22%, corresponding to 72% recovery, at 300 bar and 40 degrees C and at 400 bar and 80 C. The highest oxidation stability corresponding to 2.16 mM Ed Vit E was obtained at 300 bar and 80 degrees C. (C) 2011 Elsevier B.V. All rights reserved.
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