Journal
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
Volume 52, Issue 28, Pages 9538-9543Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ie401562j
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- Research Council of Hakim Sabzevari University
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Different aliphatic and aromatic aldehydes such as isobutyraldehyde, ethanal, n-propanal, n-butanal, n-hexanal, n-octanal, and substituted benzaldehydes were cyclotrimerized into their corresponding 2,4,6-trialkyl-1,3,5-trioxanes in the presence of commercial bulk zinc oxide at room temperature under neat conditions within a short span of time with high yield and excellent selectivity. Liquid products were formed as a separate phase and were decanted easily, whereas solid products were isolated by simple extraction. Effect of different additives, mol % of catalyst, kind of substrate, and reaction temperature were examined on the progress of cyclotrimerization reaction.
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